9781334631160 - standard reference materials (classic reprint): feasibility study for the development of standards using differential scanning calorimetry: ... scanning calorimetry (classic reprint) de callanan, jane e. (3 resultados)

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Paperback. Condición: New. Print on Demand. This book offers unprecedented insight into the development of temperature and enthalpy standards using differential scanning calorimetry (DSC). It begins by examining the advantages of DSC and its role in a world with fewer adiabatic calorimeters and less precision calorimetry. The au…thor explains that standards made by methods such as adiabatic or drop calorimetry are impractical because of the number and variety of standards required, the associated expense, and the lack of facilities and personnel to do the certification. The book outlines the study designed to evaluate the capability of a differential scanning calorimeter for developing temperature and enthalpy of fusion standards. It also explores how ASTM procedures can be applied for temperature and heat flow calibration. The author goes into detailed explanations about the statistical analysis used to determine instrument precision and accuracy, variability due to the remounting of the specimen, operator-induced variability, and weighing and analytical procedures. This book is a valuable resource for researchers and professionals working in thermal analysis. It provides comprehensive information on the use of DSC for developing temperature and enthalpy standards. This book is a reproduction of an important historical work, digitally reconstructed using state-of-the-art technology to preserve the original format. In rare cases, an imperfection in the original, such as a blemish or missing page, may be replicated in the book. print-on-demand item.