T�tulo: Phosphorus-31 NMR Spectroscopy: A Concise Introduction for the Synthetic Organic and Organometallic Chemist
Editor: Springer
Fecha de publicaci�n: 2008
Idioma: Ingl�s
ISBN 10: 3540791175
ISBN 13: 9783540791171
Encuadernaci�n: Encuadernaci�n de tapa blanda
Estado: New

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Sinopsis

The book is intended for an audience already familiar with proton and carbon NMR and commencing research in phosphane chemistry (broadly defined). It is the primary aim of this book to enable the reader to identify the main factors governing the phosphorus chemical shift values in the 31P-NMR spectrum and to make an educated guess as to where the phosphorus resonance(s) of a given target compound can be expected. It is not within the scope of this book to enable one to predict a phosphorus chemical shift precisely or even within a reasonable margin of error, with a few notable exceptions. The further intent of this book is to assist the reader in determining important issues like bond order, p-bonding contributions from substituents, the existence or non-existence of metallacycles etc. in short, to make structural assignments without the aid of X-ray crystal structure determinations and to explain structural differences in solution and the solid state where appropriate.

Cr�ticas

Aus den Rezensionen:

"... ein kompaktes Lehrbuch zur Phosphor-31-NMR-Spektroskopie. Aufbauend auf Grundwissen, das der Leser zu NMR ... haben muss, werden ... die spezifischen Eigenheiten des Phosphorkerns erl�utert. ... Das Gewicht des Buches liegt eindeutig auf einer klaren und exakten, gut lesbaren Einf�hrung zu den unterschiedlichsten Phosphorhaltigen organischen Verbindungen. Hier muss anerkannt werden, dass der Autor eine grosse Bandbreite an Strukturen und Komplexen und die Auswirkungen auf die chemische Verschiebung sehr gut bespricht. ... Die unterschiedlichen Kopplungen werden ... gut erkl�rt und Werte f�r Kopplungen im Text erw�hnt ..." (http://www.organische-chemie.ch/buecher/besprechungen/3540791175.shtm)

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