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Multi-Scale Modeling and Controlled Synthesis of Titania Nanoparticles - Tapa blanda

Akindeju, Michael

 
9783843363822: Multi-Scale Modeling and Controlled Synthesis of Titania Nanoparticles
Tapa blanda
ISBN 10: 384336382X ISBN 13: 9783843363822
Editorial: LAP LAMBERT Academic Publishing, 2014

Sinopsis

The Chemical and Manufacturing Industry is expected to benefit from the results of this work which proposed and implemented a tailor-made scheme for the continuous synthesis of Titania nanoparticles to develop a process with improved energy efficiency, predictable particle size, narrower size distribution, polymorph selectivity, and better controllability. The study investigated and modelled six polymorphs of Titania: Rutile, Anatase, Brookite, high-pressure Brookite, the columbite-type TiO2-II and Corundum-like type CLT, under constant pressure. The simulated thermodynamic, mechanical and optical properties compared favourably with known references and were used to simulate stable optimized nanoparticles. The simulated properties were used as parameters to model the network reactor system comprising of a spinning disc in the aerosol reacting volume, CSTR in the “sol” volume and settling volume according to the two-step reaction chemistry for precipitating TiO2 in a pilot scale set-up was used to validate the simulated results. The results led to an overall conclusion that the SD-CSTR is a more efficient reactor mode for the continuous synthesis of TiO2.

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Reseña del editor

The Chemical and Manufacturing Industry is expected to benefit from the results of this work which proposed and implemented a tailor-made scheme for the continuous synthesis of Titania nanoparticles to develop a process with improved energy efficiency, predictable particle size, narrower size distribution, polymorph selectivity, and better controllability. The study investigated and modelled six polymorphs of Titania: Rutile, Anatase, Brookite, high-pressure Brookite, the columbite-type TiO2-II and Corundum-like type CLT, under constant pressure. The simulated thermodynamic, mechanical and optical properties compared favourably with known references and were used to simulate stable optimized nanoparticles. The simulated properties were used as parameters to model the network reactor system comprising of a spinning disc in the aerosol reacting volume, CSTR in the "sol" volume and settling volume according to the two-step reaction chemistry for precipitating TiO2 in a pilot scale set-up was used to validate the simulated results. The results led to an overall conclusion that the SD-CSTR is a more efficient reactor mode for the continuous synthesis of TiO2.

Biografía del autor

Dr Michael Akindeju was born in Nigeria. He was educated in both Nigeria and Australia; held several process engineering and academic positions, completed his Maters and PhD by research in Chemical Engineering. He presented and published peer reviewed papers based on his findings in Australia, Malaysia, Canada, USA and Greece.

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Editorial
LAP LAMBERT Academic Publishing
Año de publicación
2014
Idioma
Inglés
ISBN 10 
384336382X
ISBN 13 
9783843363822
Encuadernación
Tapa blanda
Número de páginas
196
Contacto del fabricante
no disponible
Persona responsable
info@bod.de
info@bod.de

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