NMR Spectroscopy: Basic Principles, Concepts and Applications in Chemistry

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9783527330003: NMR Spectroscopy: Basic Principles, Concepts and Applications in Chemistry

Nuclear magnetic resonance (NMR) spectroscopy is one of the most powerful and widely used techniques in chemical research for investigating structures and dynamics of molecules. Advanced methods can even be utilized for structure determinations of biopolymers, for example proteins or nucleic acids. NMR is also used in medicine for magnetic resonance imaging (MRI). The method is based on spectral lines of different atomic nuclei that are excited when a strong magnetic field and a radiofrequency transmitter are applied. The method is very sensitive to the features of molecular structure because also the neighboring atoms influence the signals from individual nuclei and this is
important for determining the 3D-structure of molecules.

This new edition of the popular classic has a clear style and a highly practical, mostly non-mathematical approach. Many examples are taken from organic and organometallic chemistry, making this book an invaluable guide to undergraduate and graduate students of organic chemistry, biochemistry, spectroscopy or physical chemistry, and to researchers using this well-established and extremely important technique. Problems and solutions are included.

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About the Author:

Harald G�nther studied Chemistry at the Universities of Stuttgart and Heidelberg, Germany, followed by a Postdoctoral Fellowship at Mellon
Institute, Pittsburgh, USA. He then became an assistant at the Institute of Organic Chemistry at the University of Cologne, Germany, where he also completed his habilitation. He became Professor of Organic Chemistry at the University of Cologne in 1970, and at the University of Siegen, Germany, in 1978.

Review:

“Few good textbooks on NMR Spectroscopy are available at either the undergraduate or graduate levels.  For those who want to go beyond elementary organic chemistry but without delving into all the mathematics Friebolin’s book is probably the best among this category.”  (Journal of Chemical Education, 5 June 2014)

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Descripción Wiley-VCH Verlag GmbH. Paperback. Estado de conservación: new. BRAND NEW, NMR Spectroscopy: Basic Principles, Concepts and Applications in Chemistry (3rd Revised edition), Harald Gunther, Nuclear magnetic resonance (NMR) spectroscopy is one of the most powerful and widely used techniques in chemical research for investigating structures and dynamics of molecules. Advanced methods can even be utilized for structure determinations of biopolymers, for example proteins or nucleic acids. NMR is also used in medicine for magnetic resonance imaging (MRI). The method is based on spectral lines of different atomic nuclei that are excited when a strong magnetic field and a radiofrequency transmitter are applied. The method is very sensitive to the features of molecular structure because also the neighboring atoms influence the signals from individual nuclei and this is important for determining the 3D-structure of molecules. This new edition of the popular classic has a clear style and a highly practical, mostly non-mathematical approach. Many examples are taken from organic and organometallic chemistry, making this book an invaluable guide to undergraduate and graduate students of organic chemistry, biochemistry, spectroscopy or physical chemistry, and to researchers using this well-established and extremely important technique. Problems and solutions are included. Nº de ref. de la librería B9783527330003

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Descripción Estado de conservación: New. Publisher/Verlag: Wiley-VCH | Basic Principles, Concepts and Applications in Chemistry | Nuclear magnetic resonance (NMR) spectroscopy is one of the most powerful and widely used techniques in chemical research for investigating structures and dynamics of molecules. Advanced methods can even be utilized for structure determinations of biopolymers, for example proteins or nucleic acids. NMR is also used in medicine for magnetic resonance imaging (MRI). The method is based on spectral lines of different atomic nuclei that are excited when a strong magnetic field and a radiofrequency transmitter are applied. The method is very sensitive to the features of molecular structure because also the neighboring atoms influence the signals from individual nuclei and this isimportant for determining the 3D-structure of molecules.This new edition of the popular classic has a clear style and a highly practical, mostly non-mathematical approach. Many examples are taken from organic and organometallic chemistry, making this book an invaluable guide to undergraduate and graduate students of organic chemistry, biochemistry, spectroscopy or physical chemistry, and to researchers using this well-established and extremely important technique. Problems and solutions are included. | PREFACEINTRODUCTIONLiteratureUnits and ConstantsPART I: Basic Principles and ApplicationsTHE PHYSICAL BASIS OF THE NUCLEAR MAGNETIC RESONANCE EXPERIMENTThe Quantum Mechanical Model for the Isolated ProtonClassical Description of the NMR ExperimentExperimental Verification of Quantized Angular Momentum and of the Resonance EquationThe NMR Experiment on Compact Matter and the Principle of the NMR SpectrometerMagnetic Properties of Nuclei beyond the ProtonTHE PROTON MAGNETIC RESONANCE SPECTRA OF ORGANIC MOLECULES - CHEMICAL SHIFT AND SPIN - SPIN COUPLINGThe Chemical ShiftSpin - Spin CouplingGENERAL EXPERIMENTAL ASPECTS OF NUCLEAR MAGNETIC RESONANCE SPECTROSCOPYSample Preparation and Sample TubesInternal and External Standards; Solvent EffectsTuning the SpectrometerIncreasing the SensitivityMeasurement of Spectra at Different TemperaturesPROTON CHEMICAL SHIFTS AND SPIN - SPIN COUPLING CONSTANTS AS FUNCTIONS OF STRUCTUREOrigin of Proton Chemical ShiftsProton - Proton Spin - Spin Coupling and Chemical StructureTHE ANALYSIS OF HIGH-RESOLUTION NUCLEAR MAGNETIC RESONANCE SPECTRANotation for Spin SystemsQuantum Mechanical FormalismThe Hamilton Operator for High-Resolution Nuclear Magnetic Resonance SpectroscopyCalculation of Individual Spin SystemsTHE INFLUENCE OF MOLECULAR SYMMETRY AND CHIRALITY ON PROTON MAGNETIC RESONANCE SPECTRASpectral Types and Structural IsomerismInfluence of Chirality on the NMR SpectrumAnalysis of Degenerate Spin Systems by Means of 13C Satellites and H/D SubstitutionPART II: Advanced Methods and ApplicationsTHE PHYSICAL BASIS OF THE NUCLEAR MAGNETIC RESONANCE EXPERIMENT.The NMR Signal by Pulse ExcitationRelaxation EffectsPulse Fourier-Transform (FT) NMR SpectroscopyExperimental Aspects of Pulse Fourier-Transform SpectroscopyDouble Resonance ExperimentsTWO-DIMENSIONAL NUCLEAR MAGNETIC RESONANCE SPECTROSCOPYPrinciples of Two-Dimensional NMR SpectroscopyThe Spin Echo Experiment in Modern NMR SpectroscopyHomonuclear Two-Dimensional Spin Echo Spectroscopy: Separation of the Parameters J and d for Proton NMR SpectraThe COSY Experiment - Two-Dimensional 1H,1H Shift CorrelationsThe Product Operator FormalismPhase CyclesGradient Enhanced SpectroscopyUniversal Building Blocks for Pulse SequencesHomonuclear Shift Correlation by Double Quantum Selection of AX Systems - the 2D-INADEQUATE ExperimentSingle-Scan 2D NMRMORE 1D AND 2D NMR EXPERIMENTS: THE NUCLEAR OVERHAUSER EFFECT - POLARIZATION TRANSFER - SPIN LOCK EXPERIMENTS - 3D NMRThe Overhauser EffectPolarization Transfer ExperimentsRotating Frame ExperimentsMultidimensional NMR ExperimentsCARBON-13 NUCLEAR MAGNETIC RESONANCE SPECTROSCOPYHistorical Development and the Most Important Areas of ApplicationExperimental A. Nº de ref. de la librería K9783527330003

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