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Mo Molybdenum: M-o / A-B / B / 5 (Gmelin Handbook of Inorganic and Organometallic Chemistry - 8th edition) - Tapa dura

 
9783540936039: Mo Molybdenum: M-o / A-B / B / 5 (Gmelin Handbook of Inorganic and Organometallic Chemistry - 8th edition)
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Reseña del editor:
In the first part of this volume the nitrogen-containing compounds of molybdenum are described. The Mo-N system shows that M0 N and MoN are the stable nitrides. MOlybdenum 2 metal dissolves nitrogen to some extent but only at high temperatures. To get better insight into the reactions between nitrogen and molybdenum, the solubility, diffusion, adsorption and desorption phenomena, and ion bombardment are included in the section of the Mo-N system. M0 N has a large range of homogeneity toward lower nitrogen concentrations. The black 2 hexagonal MoN has only a narrow range of homogeneity. In addition some molybdenum compounds containing nitrogen and oxygen are known. The second part contains a full description of the compounds of molybdenum with fluorine. The fluorides MoF n with n ~ 2 are metastable while those with n = 3 to 6 are stable and have been observed in the Mo-F system. Pure MoF can exist without traces of oxygen, in co nt rast 3 to earlier assumptions. MoF was unambigously prepared and characterized in 1957. Its crystal 4 structure is still unknown. MoF is often contaminated with the oxide fluoride MoOF and it is s 4 difficult to remove. Even sm all amounts affect the properties of MoF . MoF , which is liquid at s 6 room temperature and solidifies to a "plastic" crystal modification below ca. 17SC, is the most investigated of all the molybdenum fluorides.
Reseña del editor:
The present volume continues the edition of a number of supplement volumes dealing with the elements tungsten and molybdenum. The compounds of molybdenum with noble gases, hydrogen and oxygen, anhydrous antimo- ny-, bismuth- and alkalimolybdates as well as compounds of molybdenum oxides with oxides of other metals have been described in volume B 1 and B 2. The oxide hydrates and the molybdate ions are dealt with in volume B 3a and B 3b. The volume molybdenum supplement B 4 contains the hydrous oxocompounds of the metals Sb to Cr with molybdenum. Description of the element molybdenum is covered by the supplement volumes A 1, A 2a, A 2b and A 3. In the first part of the volume the nitrogen-containing compounds are described. The Mo-N system shows Mo2N and MoN as the stable nitrides. Molybdenum metal dissolves nitrogen to some extent but only at high temperatures. The second part contains the description of the compounds of molybdenum with fluorine. Studies of their physical and chemical properties are complicated by the high sensitivity to traces of water resulting in the formation of oxide fluorides. These and the oxofluoromolybdate ions are discussed in separate sections. In the last part the molybdenum chlorides MoCln with n = 1 to 6 are described. The molybdenum chlorine compounds containing additional elements will be described in the following volume.

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9780387936031: Gmelin Handbook of Inorganic and Organometallic Chemistry - 8th Edition Element M-O Mo. Molybddn. Mo

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