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Sinopsis
Organic Structure Determination Using 2-D NMR Spectroscopy: A Problem-Based Approach, Second Edition, provides an introduction to the use of two-dimensional (2-D) nuclear magnetic resonance (NMR) spectroscopy to determine organic structure. The book begins with a discussion of the NMR technique, while subsequent chapters cover instrumental considerations; data collection, processing, and plotting; chemical shifts; symmetry and topicity; through-bond effects; and through-space effects. The book also covers molecular dynamics; strategies for assigning resonances to atoms within a molecule; strategies for elucidating unknown molecular structures; simple and complex assignment problems; and simple and complex unknown problems. Each chapter includes problems that will enable readers to test their understanding of the material discussed.
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Acerca del autor
Jeffrey H Simpson, PhD, was Director of the Instrumentation Facility in the Department of Chemistry at M.I.T. from 2006 to 2017. Dr. Simpson’s career in NMR/instrumentation research and instruction spans 20 years, and he has authored an introductory text on the subject of NMR as well as publishing a number of peer-reviewed articles. He is one of the Founding Members of the New England NMR Society and served as VP from its inception to 2017. He currently is a faculty member in the Department of Chemistry at the University of Richmond.
De la contraportada
Ideal for advanced undergraduate and graduate courses in organic spectroscopy, this book provides the analytical skills and methodologies needed to assign nuclear magnetic resonances to known and unknown molecular structures. Part I covers the essential knowledge along with worked examples synthetic organic chemists should possess to understand and apply NMR in their research. Part II presents a comprehensive selection of 40 problems (20 knowns and 20 unknowns), consisting of 1H and 13C 1-D spectra plus multiple 2-D spectra.
While most books on the subject focus on mathematically rigorous treatments, this text balances rigor with guidance, providing novice and experienced chemists with the tools needed to understand and interpret 2-D NMR spectra.
? Optimizes workflow by presenting strategies for assigning resonances to known structures and for deducing structures of unknown organic molecules based on their NMR spectra
? Improves analytical and interpretation skills through the use of extensive examples and problem-solving techniques
? Enhances understanding through detailed explanations of key concepts, including an extensive glossary
To learn more or see related titles, visit http://elsevierdirect.com.
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Organic Structure Determination Using 2-D NMR Spectroscopy: A Problem-Based Approach
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Academic Press, 2012
ISBN 10: 0123849705
ISBN 13: 9780123849700
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Organic Structure Determination Using 2-D NMR Spectroscopy: A Problem-Based Approach
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Taschenbuch. Condición: Neu. This item is printed on demand - it takes 3-4 days longer - Neuware -Organic Structure Determination Using 2-D NMR Spectroscopy: A Problem-Based Approach, Second Edition, is a primary text for a course in two-dimensional (2-D) nuclear magnetic resonance (NMR) techniques, with the goal to learn to identify organic molecular structure. It presents strategies for assigning resonances to known structures and for deducing structures of unknown organic molecules based on their NMR spectra. The book begins with a discussion of the NMR technique, while subsequent chapters cover instrumental considerations; data collection, processing, and plotting; chemical shifts; symmetry and topicity; through-bond effects; and through-space effects. The book also covers molecular dynamics; strategies for assigning resonances to atoms within a molecule; strategies for elucidating unknown molecular structures; simple and complex assignment problems; and simple and complex unknown problems. Each chapter includes problems that will enable readers to test their understanding of the material discussed. The book contains 30 known and 30 unknown structure determination problems. It also features a supporting website from which instructors can download the structures of the unknowns in selected chapters, digital versions of all figures, and raw data sets for processing. This book will stand as a single source to which instructors and students can go to obtain a comprehensive compendium of NMR problems of varying difficulty. Presents strategies for assigning resonances to known structures and for deducing structures of unknown organic molecules based on their NMR spectra Contains 30 known and 30 unknown structure determination problems Features a supporting website from which instructors can download the structures of the unknowns in selected chapters, digital versions of all figures, and raw data sets for processing 540 pp. Englisch. Nº de ref. del artículo: 9780123849700
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